Experimental study of microhardness of glass ionomer cements and E-max MT ceramics compared to primary tooth enamel
https://doi.org/10.33667/2078-5631-2025-20-90-93
Abstract
Background. The study of microhardness of dental materials, especially those used in pediatric dentistry, is an important task in modern dentistry. Glass ionomer cements (GICs) and E-max MT ceramics are widely used for tooth restoration, but their mechanical properties compared to primary tooth enamel remain understudied.
Objective. To evaluate the microhardness of glass ionomer cements (Fuji-9, Vitremer) and E-max MT ceramics in comparison with primary tooth enamel.
Materials and methods. Laboratory tests were performed on 25 samples of each material.
Microhardness was measured using a manual digital press RPG-75. Statistical analysis included Shapiro – Wilk, Levene, Bartlett, Kruskal-Wallis, and Dunn tests (p < 0.05).
Results. Primary tooth enamel exhibited microhardness of 1.97 ± 0.22 kN, surpassing GICs (Fuji-9: 1.11 ± 0.15 kN; Vitremer: 1.36 ± 0.07 kN) but remaining inferior to E-max MT ceramics (8.03 ± 0.71 kN). Intergroup differences were statistically significant (p < 0.05).
Conclusion. E-max MT ceramics show the highest strength, making them suitable for load-bearing restorations. GICs, while less durable than natural enamel, offer advantages in biocompatibility and anti-caries effects, which are critical in pediatric dentistry.
About the Authors
E. R. RubininaRussian Federation
Evrina R. Rubinina – Applicant for Degree at the Department of Clinical Dentistry with Courses in Surgical Dentistry and Maxillofacial Surgery
Pyatigorsk
R. D. Yusupov
Russian Federation
Ruslan D. Yusupov – MD, PhD, Professor of the Department of Clinical Dentistry with Courses in Surgical Dentistry and Maxillofacial Surgery; Leading Researcher at the Head and Neck Medical Laboratory
Pyatigorsk
Grozny
T. V. Simonyan
Russian Federation
Tatyana V. Simonyan – MD, PhD, Associate Professor, Head of the Department of Clinical Dentistry with Courses in Surgical Dentistry and Maxillofacial Surgery
Pyatigorsk
M. R. Yusupov
Russian Federation
Muslim R. Yusupov – 5th-year student
Pyatigorsk
I. N. Kukishvili
Russian Federation
Ilona N. Kukishvili – Clinical Resident at the Department of Pediatric Dentistry with Continuing Professional Education Course
Pyatigorsk
S. V. Voronina
Russian Federation
Svetlana V. Voronina – PhD in Technical Sciences, Associate Professor
Pyatigorsk
References
1. Votyakov S.L., Mandra Yu.V., Kiseleva D.V., Vlasova M.I. Clinical and experimental evaluation of the use of nano-filled glass ionomer cement Ketac N-100 for aesthetic and functional dental restorations. Ural Medical Journal. 2008;(10):93–97. (In Russ.)
2. Murashkina M.V., Danilova E.A. Comparative characteristics of the treatment of primary teeth with glass ionomer cements in children aged 5-6 years with II-III degree of caries activity with and without the use of Gluma. In: Current Problems of Experimental and Clinical Medicine. 71st Open Scientific and Practical Conference of Young Scientists and Students of VolgSMU with International Participation. 2013. Pp. 153–154. (In Russ.)
3. Goryainova K.E., Rusanov F.S., Poyurovskaya I.Ya., Retinskaya M.V., Lebedenko I.Yu. Comparative evaluation of the strength of dental materials for chairside CAD/ CAM technology. Russian Dental Journal. 2016;20(3):116–120. (In Russ.)
4. Kolodkina V.I., Arutyunov A.V. Morphological structure of tooth enamel, dentin and composite restorative materials in vitro. Russian Dental Journal. 2018;22(4): 176–179. (In Russ.)
5. Tishkov D.S. Analysis of flexural strength and porosity of high-powder liquid and resin-modified glass ionomer cements. Regional Bulletin. 2020;(8):6–7. (In Russ.)
6. Furmann D., Merkison D., Whipple S., Vandewalle K. Properties of novel glass ionomer restorative systems designed for stress-bearing areas. Oper Dent. 2020;45(1):104-110. doi:10.2341/18-176-L.
7. Chen X., Gu L., Liao B., Zhou S., Cheng L., Ren B. Advances in anti-caries nanomaterials. Molecules. 2020;25(21):5047. doi:10.3390/molecules25215047.
8. Jandt K.D., Watts D.C. Nanotechnology in dentistry: Present and future perspectives on dental nanomaterials. Dent Mater. 2020;36(11):1365–1378. doi:10.1016/j.dental.2020.08.006.
9. Shalamay L.I., Mendoza E.Yu., Mayorov E.E., Lampusova V.B., Oksas N.S. Study of the latest dental materials using tensile testing to determine tensile strength. Proceedings of Higher Educational Institutions. Instrument Engineering. 2022; 65(8):612–618. (In Russ.)
10. Mayorov E.E., Mendoza E.Yu., Shalamay L.I., Oksas N.S., Lampusova V.B. Determination of the physical and mechanical parameter by tensile testing in modern dental composite materials. Dental Forum. 2022;(3):29–34. (In Russ.)
11. Xiao Y., Deng L., Huang S. et al. Effect of bioaging on the mechanical properties and microbial behavior of different polymer composites. Biomolecules. 2023;13(7):1125. doi:10.3390/biom13071125.
12. Gabaydullina V.V., Kotyakov M.A., Urukov Yu.N., Moskovskiy A.V., Altsev V.V., Moskovskaya O.I. E-max crowns: metal-free ceramics. Healthcare of Chuvashia. 2023;(4):87–90. (In Russ.)
Review
For citations:
Rubinina E.R., Yusupov R.D., Simonyan T.V., Yusupov M.R., Kukishvili I.N., Voronina S.V. Experimental study of microhardness of glass ionomer cements and E-max MT ceramics compared to primary tooth enamel. Medical alphabet. 2025;(20):90-93. (In Russ.) https://doi.org/10.33667/2078-5631-2025-20-90-93